Step 9Separate the toluene layer
Repeat by adding another "shot" of toluene to the catnip water in the nalgene bottle. Shake it up really well, let it separate, and use the turkey baster to suck off the top layer, placing it into shot glasses. When you're done you might end up like me with an array of shot glasses, mixed with toluene/water.
The mechanical action of transferring the liquid to shot glasses seems to help the layers separate further. The ultimate goal is to get rid of the water layer entirely, giving a clear toluene solution.
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