How to Make a Synthetic Diamond

How to Make a Synthetic Diamond
My 10-year Wedding Anniversary is coming up so I thought I'd make my wife something special. A few months back I'd seen a show on TV where they demonstrated how companies were now making "cultured" diamonds in the lab. There are a few different methods, but the simplest is something called "chemical vapor distillation". The process is pretty straightforward. Basically, microwaves are used to create a slurry of graphite plasma which, when rapidly cooled form a crystal structure.

I checked around on the internet and found several sites where others have been doing the same thing. The best part was that everything I'd need were pretty common household items. So, I rounded up the necessary supplies and began imagining how great life would be once I'd cornered the international diamond market.
 
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Step 1Materials

Materials
Here's the surprisingly short list of materials I used:

A standard home microwave oven
2 coffee mugs
3 pieces of 3mm graphite pencil lead
A few drops of extra virgin olive oil
A 5" piece of 100% cotton thread

The hardest item to find was the 100% cotton thread. It's amazing how scarce that stuff is. After searching through all of our sewing notions, I finally found some black thread that I think my mom bought back in the 70's.
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328 comments
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Jan 10, 2012. 12:19 AM1161858 says:
you sir are an alchemist hahaha
Mar 9, 2010. 9:01 AMnotosalvation says:
This is by far my favorite article I have read on this site. At the same time it only diminishes my faith in humanity. I truly applaud your wit and creativity.
Oct 28, 2011. 3:03 PMlwhybrow says:
Dude you are so cool!!! I love this article and I will tell all my friends about it!!
Dec 16, 2009. 9:38 AMlesley090 says:
so exactly how long do you need to have it the microwave
Oct 11, 2011. 4:59 PMmcuz says:
Hey, can you please make a video of this and put it on youtube?
Dec 16, 2009. 11:10 AMlesley090 says:
ok but does experiment actually work and how would the crytals come out to be
Jan 28, 2012. 8:23 PMpopewill says:
very
very
very
interesting,
my
friend
Sep 12, 2011. 12:03 AMvwan says:
this is all bull!!!! there are NO ways to create a synthetic diamond with household objects!!!!!!!!!
the only way to create a synthetic diamond in a few minutes, is to create an explosion soooooooooo strong the graphite will pressurize into diamond.
FULL STOP
and that will only give you about 25 to 30 cents of diamond.
HAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHA
AHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHAHA
lol rofl!!! ahahahahahahahahahahaha
Oct 6, 2011. 2:37 PMmbowman5 says:
Ah...But you can make a fake diamond in your garage...not using household items though. Im a Diffusion Engineer in the semiconductor industry. I work with LPCVD toolset.. Low Pressure Chemical Vapor Deposition. Making diamonds uses CVD also. What you would need is to figure out whether you need the process to be under vacuum, hence the Low Pressure. Find a used CVD chamber off a used Applied Materials tool. Im sure a 2" or 4" wafer chamber size will do just fine. These are probably cheap too if you can find them since nobody uses them anymore. You'll need a gas delivery system for gases Methane and Hydrogen. A safety net too for the hydrogen since its highly flammable. So you can use an old Edwards standard vacuum pump to pump down to 10 to the -8th Torr, The chamber must be heated to 1300 degrees, figure out if C or F first. then gases need to be injected for a predetermined amount of time. Process takes 12 hours. You will most likely need a 480v outlet too since most tools run off of 480V. I've heard of people having a small fab setup in their garage. Your electric bill will skyrocket too! Dont forget you need a baby pure diamond to start with. So its feasible just not practical
Jun 25, 2011. 11:11 AMSMarshall14 says:
would it work better if you crushed the graffite up in a pessle and motor than mixed in the oil leave to soak then absorb the oil (with clothe ) then place in the path of sevral MASERs
Jun 19, 2011. 5:35 PMtinker234 says:
wow thanks hey is it a real dimond because if it is i can be very rich just selling them
May 4, 2011. 5:11 PMKama Amak says:
My mother just dies and i would like to crush her carbon remains into a few nice gems.
Please can any help me withthis process?
I saw on lifegems that it is areound 3000 - 250000 to do this. I can not afford this but i need to do this.
Can i do tis in my garage?
Thanks Kama
admin@myfloridakids.org
Jun 19, 2011. 5:33 PMtinker234 says:
im sorry for your loss hey you know im not sure if this works
Apr 3, 2010. 9:15 PMCheathum14 says:

I don't like being "that guy" but it seems there are plenty of others on this site so im going to say it anyway; thats not a diamond. Here are a few reasons why.
1. The pencil lead you used contains a large amount of clay, not just graphite.
2. Microwaves are not capable of generating the heat neccesary to recrystalize carbon.
3. Even if the microwave could reach the neccessary temperature, the pressure required to make a diamond is around 50,000 to 70,000 times that of earth's atmosphere.
4. How is it that you claim to have made a diamond in your microwave if diamonds weren't even synthesized until 1953, six years after the first microwave oven was made? If they had the technology in 1947, why not use it then?

Sorry for pooping your party, but it looks like im not the only one.

Apr 30, 2011. 9:35 PMKimberlyP says:
http://patft.uspto.gov/netacgi/nph-Parser?Sect1=PTO2&Sect2=HITOFF&p=1&u=%2Fnetahtml%2FPTO%2Fsearch-bool.html&r=0&f=S&l=50&TERM1=Apollo+Diamond&FIELD1=ASNM&co1=AND&TERM2=&FIELD2=&d=PTXT

Apollo Diamond

You could use a microwave and an Absorber such as Silicon Carbide to absorb the microwave radiation and convert to heat.

You would need much lower pressures but you would have to have a controlled atmosphere to the Silicon carbide chamber and that chamber would have to have a suitable refractory and need to be kept cool such that its heat up does not cause ionization which results in it absorbing microwaves and heating up as well.

Apollo Diamonds are gem perfect they can only be identified by lack of any defects. Of Course if done at home you could vary input defects theoretically and they could never be identified.

Microwaves are ideal in this process because of the tight control of temperature in connection with the absorber. It is also more energy efficient.

Apr 30, 2011. 9:16 PMKimberlyP says:
Microwaves with a suitable absorber. Silicon Carbide, Zirconium Oxide, Plutonium Oxide and others, can absorb nearly 100% of microwave radiation.

They heat up and radiate in infrared. You need a suitable refractory and you probably want to keep it cool so that it does not heat up and ionize and start absorbing microwave energy.

The temp is achievable.

For small crystals you could use cavitation and therefore not need the high pressures. The crystals would be very small.

For Large crystals you need not have as high a pressure but you do need a controlled atmosphere.

They were using microwaves as early as 1953 at Y-12 to deal with radioactive materials processing.

You may have made Silicon Carbide in a process similar to the Acheson Process if you arced in non controlled atmosphere.
http://en.wikipedia.org/wiki/Silicon_carbide
Jan 29, 2011. 3:13 AMbarkbark says:
About the microwave..I'm thinking that a discovery of diamond-making need not come out the second the microwave is launched..people were pretty freaked by them.. Microwaves for food uses anyway because they were scary..
Hitler refused to allow his troops to eat food cooked it them because they were proven to mutate protein, and mutant proteins become cancerous, still a researched and proven fact, the old documents are still around for public review, online. Microwaves were around in studies years before they were launched, but they recieved passage into the public through a manipulative buy-off, against the will and recommendation of the reviewing doctors of the day on the panels.

So heads were not all about playing with microwaves in popular masses. A few were daring to launch experiments, but its main intention had some sinister purposes even though it was promoted for cool ones. Diamonds on the other hand would've been a lighter area of creative experimentation, dangerous as all science can be. I wish I'd known about the diamond thing earlier--it would've been fun to work with :D! Glad I no longer use a micro, though..
Apr 28, 2010. 4:57 AMTreknology says:
Let me bomb your party.

1. A real diamond placed in a CO2 atmosphere will dissolve into "nothing"--no pressure or heat involved.

2. Fake industrial diamond is not manufactured under such high temperatures or pressures either.

3. An Australian high-school student developed a way of coating materials in diamond micro-dust, using COLD and low pressures--great for making grinding wheels but hopeless for laser focusing devices.

Superheat and pressure is only theory.
Oct 26, 2010. 1:33 PMzoteman94 says:
It isn't only theory, graphite is the most stable allotrope of carbon at ambient temperature and 1atm pressure. (Yes you can convert diamond into graphite in an inert atmosphere at around 1000°C) Maybe there are some ways that don't need ultra high temperatures or pressures, but it is proven that diamond is more stable than graphite at these conditions and thats why it transforms into it.
May 9, 2010. 2:04 PMCheathum14 says:
@Teknology
You didn't quite bomb my party. I know that diamonds can be formed at much lower temperatures and pressure.(Microscopic diamonds can form on the surface of the sun where the temp. is only 10,000 and where there is little pressure) I was just saying that for a diamond of that size (visible to the naked eye) to be formed, it would take more than the pressure and heat a microwave can generate. Also, if i'm wrong, so be it, i'm only a sophomore in high school anyway and i'm taking physics next year.
Apr 29, 2010. 5:46 AMTreknology says:
I was bombing Cheathum14, not you. But I do re-assert that extreme heat and pressure will not be the methods by which "gem" quality diamonds are reproduced--and even then they won't be "gem" quality because they will lack the unique flaws of the natural product.

Of course, if subsequently worthless "pure" diamond can be grown then lenses and other optics will take a massive left turn in efficiency. And yes, I confidently predict that such method will not only validly suck carbon out of the atmosphere, it will turn out rocks in such volume that the South African economy will collapse.
Jan 14, 2011. 7:57 PMmogg says:
Synthetic diamonds are made at about 300deg C, but usually in a pressure vessel using microwave radiation and a "seeding" crystal. You can make diamond as big or small as you want by growing them in a chemically neutral environment (nobel gas/ nitrogen) using CO2. Check out wikipedia, has an article about them. The diamonds are purer than natural sourced diamonds, and are currently being applied to electronics, especially light based circuits.
Go to a big jewelers and ask for yellow diamonds- they are tinted to distinguish them natural ones, but they can come in any colour depending on the material you poison the crystals with. They have the same colour as urine.
I haven't tried it, so can't say if this will work, but I'm skeptical of the chemistry.Once I've destroyed my microwave (it's crap anyway), i'll let you know. (^^)
Apr 5, 2010. 9:31 AMCheathum14 says:

:) Well played. I thought there was something odd about this instructable. Also, pranking me isn't quite that difficult because im the most gullable guy in my county.

Apr 15, 2010. 7:00 AMaqwiz says:
 I hope you don't live in poland. 
May 9, 2010. 1:22 PMCheathum14 says:
haha, i live in texas and i'm gullable, not stupid :)
May 9, 2010. 5:53 PMaqwiz says:
 Oh my bad I misread that, thought you said country. 
Sep 24, 2010. 10:59 AMMr. Potato Head says:
Guess that makes you the stupid one!
Mar 24, 2011. 8:46 PMdombeef says:
Wow, this is really cool! I am going to try this right now, the graphite is almost done soaking, how big does it have to be? I am trying two kinds right now, 0.7 mm and 0.5mm, wish me luck!
Apr 3, 2009. 11:50 AMgothicbob says:
99 mins 99 seconds of microwaving... your electricity bill is going to be expensive if this becomes a hobby.
Mar 6, 2011. 3:21 PMAsmodeous says:
Not as expensive as a real diamond:)
Sep 21, 2009. 5:19 AMMedalya says:
i know this was a while ago but i have to say it cause no one else did. GULLIBLE!! lol microwaves have a built in safety switch, if you pulled the microwave apart (don't do it if you ever want to have kids) it would be possible to make a diamond, but you still need pressure. :)
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