Introduction: Measure Muscle Sounds! Part 2: Silicone Embedding

About: Experienced technical lead with a passion for design, usability and accessibility. Creator of tecla, the best smart hub for switch accessibility.
This is the long-awaited follow up to the super awesome Measure Muscle Sounds! instructable.

To see what you can do with these sensors, check out these videos.

Silicone embedding is the trickiest part of the process of building your own muscle sounds sensor. This is why I chose to make this a completely separate instructable. This instructable will definitely test your patience and manual ability, so be prepared to screw up a couple boards before you get the hang of it.

So without further delay... let's get started!

Step 1: Complete Part One of the Instructable

This instructable is a follow-up for the Measure Muscle Sounds! instructable published a while ago. Make sure you complete that instructable first unless you just want to try embedding something else (like your younger brother) in silicone and you just want to know how to do it.

Step 2: Bill of Materials

This instructable requires a few custom materials and tools. The lab where I made the sensors already had most of the materials/tools available or they were custom-made there, so I apologize for not being able to direct you to specific suppliers/part #. If you try the instructable, please post where you got your materials from!

Part: Nylamid spacer (Diam: 13mm, Thick: 2mm)
Supplier: Custom-machined
Qty: 1 per sensor (reusable)

Part: 20A Shore RTV Silicone
Qty: ~2g per sensor

Part: 65A Shore RTV Silicone
Qty: <1g per sensor

Part: Acrylic (transparent plastic) board with circular indentations
Specs: 25mm minimum width and length
Centered indentation depth: 0.4 - 0.6mm
Centered indentation diameter: 4 - 6mm
Additional indentations at a minimum 30mm distance in any direction
Supplier: Custom-machined
Qty: 1

Other: Assorted modeling hand tools, precision scale, metal roller, silicone solvent.

NOTE: You can get the silicone and solvent from Nusil Technology. The modeling tools, you can probably find in a good art supplies store.

Step 3: Glue the Spacer on the Microphone

As seen in the picture below, the microphone must be coupled to a sealed air chamber directly underneath it. In order to achieve this, we need to embed the whole thing in silicone. This is done in a two step process: first, we build a case for the board making sure we leave the space for the air chamber, and second, we cover the whole thing from underneath with a silicone membrane sealing the chamber.

The air chamber is quite small (equivalent to a cylinder of 13mm in diameter and 2mm in height). This is where the nylamid spacer comes in. You need to glue the nylamid spacer directly to the microphone (figures 2 and 3). You also have to make sure the spacer is centered with the microphone. Note that the microphone is not centered on the board so the plastic spacer will be slightly offset and the board cannot be used as a reliable reference. Be careful not to let glue into the microphone because this will definitely make it useless and you will have to start all over!!. You can carefully glue a small piece of paper to the microphone first to protect it.

In terms of the glue, this is still an unresolved problem (suggestions welcomed). I have only used glue sticks because you have to make sure you will be able to remove the spacer afterwards (i.e. you need a weak glue), but if the glue is too weak, you won't be able to hold the spacer in place during embedding and the whole thing will become really difficult and frustrating. I encourage you to try a few different glues and post your results here, a glue stick is definitely NOT the best solution.

Step 4: Mix the 20A Shore Silicone

The RTV silicone comes in two parts conveniently marked "part A" and "part B". You need to mix thoroughly both parts in a 1:1 mass ratio. Try to do this in as low a temperature and as dry environment as you can. Once mixed, the silicone will start to vulcanize at room temperature (RTV stands for room temperature vulcanized) and it will become increasingly difficult to work with.

You will need about 2g total of the 20A shore silicone (i.e. 1g of part A + 1g of part B) for each sensor. If you are making more than one sensor at a time, it is ok to mix all the silicone required at once. However, once mixed, the silicone must be used ASAP. You can store the unused mixed silicone in a plastic bag in your freezer, but I don't recommend it (I would rather use the extra silicone to model something else, like a fake finger to mix with candies for halloween).

Spend a few minutes mixing the silicone with a clean metal roller in the same way you would mix pasta or cookie dough. In fact, a pasta roller may work pretty well to prepare the mix. Make sure there is no grease/oil on any of the surfaces the silicone touches. Grease will prevent the silicone from vulcanizing so wash your hands or wear surgery gloves. Also, make sure no air bubbles are left in the mix.

Step 5: Create the Silicone Case

Use some more glue to fix the nylamid spacer (with the sensor attached) on a flat surface. You can use the back of the indented acrylic platform as a flat surface. Of course, by "back" I mean the side that is not indented.

You will get a "sandwiched" spacer where the "top slice" is the sensor and the "bottom slice" is the flat surface. At this point, you are ready to start placing some of the mixed silicone all around the sensor and spacer. You want to seal every single space and make sure there will be no air bubbles trapped. Don't worry about the electronic components, they work with very low currents so they won't overheat or short-circuit even when embedded.

Start by carefully shoving small quantities of silicone in tight spaces using the different modeling tools, then pack some more silicone around those spaces. Pack tightly, especially in the space between the spacer and the PCB around the microphone, and ensure the microphone is always centered on the spacer before continuing. Repeat until the silicone shows up around the board and use a flat spatula to pack the silicone some more from all 4 sides. My cases usually end up more square than the one shown (I didn't make this one).

Also make sure to cover the whole top of the board. It is not necessary to cover the accelerometer completely, so you can use it as a reference to even out the silicone at the top. Be prepared to spend up to 2 hours in this step, lousy embedding will make your sensor useless.

Step 6: Cure (vulcanize) the Silicone Case

Place the silicone-embedded sensor into an oven at 60 deg C and allow curing for approximately eight hours. you can probably speed up the curing process with higher temperatures. However, some of the tiny air bubbles could pop and create fissures which may cause air leaks, making your sensor useless. You can actually see the air bubbles in the examples below (the silicone is not smooth and has too many reflections). This sensor was cures at 60 deg C for 8 hours, so the bubbles are probably due to lousy embedding.

After curing, carefully remove the sensor from the plastic board and then remove the plastic spacer. The case should look like the second figure below but with no bubbles!!!

Step 7: Mix the 65A Shore Silicone

Now mix some of the 65A shore silicone just as explained in step 4. This silicone will be used to create the bottom membrane that seals the case from below. You will need about 1g per sensor. In fact, you need less than this, but if you can't measure less than 1g with good precision, it will be difficult to maintain the 1:1 mix ratio, so you should go for the safer 1g measure (i.e. 0.5g of part A + 0.5g of part B) and use the remainder for the nail of your fake halloween finger.

Step 8: Roll Membrane on Indented Board

After cleaning the plastic board thoroughly, use the 65A shore silicone you just mixed and a small metal roller to produce a thin membrane centered on one of the indentations of the plastic board. Be sure to pack silicone into the indentation before flattening the membrane out. The indentation is in fact optional, but it will help secure good coupling between the skin and the sensor.

The thickness of membrane should be approximately 0.5mm, although I have no idea how to ensure this to happen (more suggestions welcome).

Step 9: Apply Solvent to Case Edges

Using a small brush, apply silicone solvent to the edge of the silicone case, on the microphone side, where it will contact the membrane. This allows the surface of the silicone to dissolve a bit to facilitate proper curing and sealing with the membrane. Also make sure the area of the membrane in the board is larger than the entire sensor case before continuing.

Step 10: Apply Membrane and Cure

Mount the sensor onto the flattened membrane making sure that the microphone is centered on the indentation in the plastic board. Use the excess silicone edge to seal the membrane onto the sensor by pulling it upwards and around the case.

Allow the sensor to cure at 60 deg C for eight hours.

Step 11: You Are Done!

After curing, your sensor will be ready for testing. In order to do that, you can tap slowly on the membrane and check the microphone's output signal. You should be able to see the wave in a scope very clearly (for details on the electronic circuit check the first part of the instructable.). The membrane should quickly restore itself when deformed, otherwise, there may be an air leak. There is no reliable solution to air leaks... your best bet is to trash that sensor and start again.

By embedding in silicone, the sensor sensitivity has been passively increased. You have also enabled the microphone to measure really low frequency vibrations such as those produced by contracting muscles. Try placing the sensor in your chest and watch/listen your heart beats!

Check out the videos:

http://www.komodoopenlab.com/index.php/Portfolio/CMASP#vids

And above all, have fun!

NOTE: The techniques presented in this instructable are not optimal and still pretty rudimentary. Some of the disadvantages include a lack of consistency in the performance and sensitivity of the sensors built (due to the lack of precision in manufacturing). You are encouraged to suggest different, easier and/or more appropriate ways to solve any of the steps of this instructable. Your input will be extremely valuable in making these sensors affordable and useful in prosthetics.