Pocket Size Spinthariscope

34,368

79

28

The spinthariscope was invented by William Crookes in 1903. While observing the apparently uniform fluorescence on a zinc sulfide screen created by the radioactive emissions (mostly alpha radiation) of a sample of radium bromide, he spilled some of the sample, and, owing to its extreme rarity and cost, he was eager to find and recover it.

Upon inspecting the zinc sulfide screen under a microscope, he noticed separate flashes of light created by individual alpha particle collisions with the screen. Crookes took his discovery a step further and invented a device specifically intended to view these scintillations.

It consisted of a small screen coated with zinc sulfide affixed to the end of a tube, with a tiny amount of radium salt suspended a short distance from the screen and a lens on the other end of the tube for viewing the screen. Crookes named his device from Greek σπινθήρ (spinth´ēr) "spark".

NOTE

What's the difference between the upgraded, and regular version? The previous version used a reflection based fixed scintillation screen, while this version uses a transmission based adjustable scintillation screen. Compared to the previous version this one offers an increased scintillation rate, and the ability to set the distance between the source and the screen.

Step 1: Safety First

To build this device you'll need to deal with a radioactive substance: Americium 241.

In the process of radioactive decay, americium releases alpha particles and gamma rays. Alpha particles are relatively high energy particles, but travel only extremely short distances and do not penetrate the skin.

However, if americium is taken into the body and enters body tissues, alpha particles may produce damage to nearby cells.

The radiation from americium is the primary cause of adverse health effects from absorbed americium. Upon entering the body by any route of exposure, americium moves relatively rapidly through the body and is deposited on the surfaces of the bones where it remains for a long time.

The dose from this alpha and gamma radiation can cause changes in the genetic material of these cells that could result in health effects such as bone cancers.

Gamma rays can travel much greater distances and can penetrate the entire body. Since alpha particles do not penetrate the skin and the gamma rays released from americium sources are relatively low in energy, external exposure to americium is not usually considered to be a danger to your health.

Anyway you must use at least eye protection, dust mask and rubber gloves when dealing with Americium 241.

Step 2: The Legal Bit

Disassembling a smoke detector

Disassembling a smoke detector to obtain the americium source may be subject to laws in your country, and that proceeding could open you to legal liability.

You must check the laws in your country before disassembling a smoke detector.

Disposal

State and local requirements for disposal of ionization smoke alarms vary. Some States conduct an annual roundup of ionization smoke detectors similar to that for hazardous household chemicals. Others allow ionization smoke detectors to be thrown out with ordinary trash but recommend that used smoke alarms be returned to the supplier. Some States require that used smoke detectors be returned to the supplier.

You must check with your local solid waste district, hazardous waste program, or health department to find out the procedures in your area.

Step 3: Materials Needed

To build this pocket size spinthariscope you will need:

...and a 3d printer. Or a friend with a 3d printer ;)

The only purpose of the ionization smoke alarm is to be disassembled to provide me the radioactive source. Now, I am not going to elaborate how ionization chamber works inside smoke alarms because it will digress from our current topic. What I was interested was extracting the radioactive source inside the smoke detector; and so I did.

Step 4: 3D Model

I designed a microscope extension to host both the radioactive source and the scintillation screen. You simply need to download the STL file and print your own extension.

Should you need to modify it just use the STEP file and import it in your design software.

Step 5: Assembly and Test

The assembly is pretty straightforward:

    • wear your gloves, eye protection and dust mask and remove the Americium 241 source from the smoke detector. You will need just the small button shown in the pictures (this instructable could help).
    • remove the light module from the microscope.
    • grab the 3D part you just printed.
    • glue the M8 nut in the hexagonal recess, it should be a tight fit so may need to push a little to get it in place.
    • glue the americium source on the tip of the M8 screw.
    • lay down some scotch tape with the sticky face facing upward, spread some ZnS powder on it and distribute it evenly.
    • cut the scotch tape to obtain a disc with a diameter of 15 mm
    • fit the disc into the 3D printed part with the sticky face (the face will not be so sticky now) in contact with the 3D printed part.
    • glue the microscope into the 3D printed part.
    • set the focus in order to get a clear view of the powder grains on the scotch tape
    • Fit the M8 screw in the M8 nut and gently screw it all in

    Put the spinthariscope in a dark place to let the powder go dark.

    Step 6: Conclusions

    Americium-241 emits mostly alpha particles (and a negligible portion of gamma emission) with average energy of 4.5 million electron volts (MeV). Each source contains less than 0.5 micrograms of americium dioxide with an activity of 0.8 microcuries which is equivalent to about 30000 nuclear disintegration per second.

    When alpha particle travel in air at great speed, in this case about 15000 kilometres per second (based on 4.5 MeV relativistic kinetic energy) it has high probability to collide with anything that comes in their way due to its relative huge size. Usually these particles don't travel far, about 4 centimeters at most in air and will lose their energy in scattering events. It is like smashing a cue ball into a pool table full of billiard balls - eventually the cue ball will stop as it deposits its kinetic energy into the surrounding ball during collisions.

    When collided in just the right way with the right materials, the passage of an alpha particle can be "seen". This is done with a process physicists call "scintillation".

    A suitable material such as ZnS:Ag or ZnS:Cu (zinc sulfide doped with silver or copper) will emit flashes of light when it is being collided by alpha particles.

    The light emitted is blue for ZnS:Ag and green for ZnS:Cu.

    I did not see anything at first but it was no surprise, because each scintillation is very faint. But when our eyes adapt to the dark, they have higher capability to detect those faint flashes of light and it will usually take about 15 to 20 minutes to reach that kind of sensitivity in darkness.

    Adjusting the position of the screw you can adjust the distance between the source and the screen. The number of scintillations will rapidly decrease if you increase the distance.

    In vacuum the scintillation density obeys an inverse square law – getting weaker with the square of distance, i.e. doubling the distance quarters the intensity. Tripling the distance leads to a ninth of the intensity. In air you need also to consider the scattering, so the scintillation density will get even weaker.

    So you did it! You juts gained a superpower! You can see the subatomic world with your bare eyes now!

    Have fun! :)

    Acknowledgement

    I'd like to tanks all the users that commented this instructable for their contribute to make it better and safer!

    Pocket Sized Contest

    This is an entry in the
    Pocket Sized Contest

    Share

      Recommendations

      • Arduino Contest 2019

        Arduino Contest 2019
      • Trash to Treasure

        Trash to Treasure
      • Tape Contest

        Tape Contest

      28 Discussions

      1
      None
      almateus

      4 days ago

      Do you think that if you attach a webcam to the microscope it would show the scintillations? That would make it easier to show what happens to the students. Thanks for the instructable. No smoke alarms here in Brazil, but I do have an Americium source at school, maybe I will try this sometime.

      5 replies
      0
      None
      Peter Balchalmateus

      Reply 1 day ago

      Remove the lens and filter from the webcam and just put the Americium near the ccd sensor. No need for ZnS. If you google for 'Americium webcam', you'll find examples.

      0
      None
      hombremagneticoalmateus

      Reply 3 days ago

      Hi almateus, the new version is more suitable to be used with a USB microscope. The scintillations are brighter using the scotch tape screen, but I don't know if a normal webcam is sensitive enough. Putting the scotch tape directly in contact with the CCD (powder side facing outwards) should do the job though...

      0
      None
      herbivore1almateus

      Reply 3 days ago

      The webcam on a microscope is an awesome idea! Or, go to ebay and search for "USB Microscope" You can get a 1.3 megapixel USB microscope with > 100x magnification for just over $10 to $12 (including shipping.)

      0
      None
      almateusherbivore1

      Reply 3 days ago

      Thanks for reminding me that I have one of those already. It basically is a webcam with a lens in front of it. Don´t know if it can magnify 100X, or if the sensor is sensitive enough for low light conditions, but it is worth a try.

      0
      None
      pemazzeialmateus

      Reply 3 days ago

      Olá, no Mercado Livre você acha alguns modelos, Não sei se usam o Americium. Grato

      0
      None
      SHOE0007

      1 day ago

      Well, Amercium 241 is cheap to get and you can get old smoke alarms on ebay for that or a smoke detector. I like this type of project. I bet other ore like Pitchblade which is 80 percent UO2 would not work since it not powerful enough alpha particles It 8000 cpm were Alpha can be 100,000 CPM in alpha.

      1
      None
      RobertS770

      Question 2 days ago

      What's the difference between the upgraded, and regular version?

      1 answer
      0
      None
      hombremagneticoRobertS770

      Answer 2 days ago

      Hi RobertS770, the previous version used a reflection based fixed scintillation screen, while this version uses a transmission based adjustable scintillation screen. Compared to the previous version this one offers an increased scintillation rate, and the ability to set the distance between the source and the screen.

      2
      None
      tercero

      6 days ago

      I LOVE this instructable. It's very cool. My wife teaches elementary school, I wonder if it would be considered safe enough for her to bring into the school to give a demonstration if I build this.
      Thanks again for this instructables.

      6 replies
      0
      None
      LeslieGeeetercero

      Reply 4 days ago

      Hi Tercero, Your wife and you probably realize this already, but considering how some people are these days, I would suggest that she run this experiment by the Principal, write up exactly what she will be doing and how the ingredients work and have the parents sign off on letting the children "participate". Accidents do happen and some kids just have an overwhelming need to touch and know why. There is always the one or two kids that have earplugs in when the word dangerous is said. Kids sometimes have no concept of danger (we were all there once :) ) and this can go terribly wrong. Good luck.

      1
      None
      terceroLeslieGeee

      Reply 2 days ago

      I finished building this, and instead used an adapter for my Nikon Z6 FX to take some pretty amazing shots.
      She showed the results to her class and explained what exactly they were looking at.
      Pretty amazing.

      0
      None
      hombremagneticotercero

      Reply 6 days ago

      Thanks! :) Well... as long as the source is not ingested or touched with bare hands it should be pretty safe. But the better people to ask for info and authorization should be school's health and safety representatives. Every country has is own laws...

      0
      None
      garybautercero

      Reply 4 days ago

      As a demo
      You need to hold it against your eye

      Not a good idea when it cannot be guaranteed to be sealed or uncontaminated.

      Even at senior physics classes this has been abandoned..as not a good idea.

      Biggest issue was eye infections from the eye piece..

      3
      None
      garybau

      4 days ago

      Illegal in Australia as well.
      Not to be encouraged.

      1 reply
      0
      None
      hombremagneticogarybau

      Reply 3 days ago

      Thanks for your comment! I added a "legal bit" section as well.

      3
      None
      Bridges-PdP

      3 days ago

      Great instructable. I sure wish all these 'Safety Pups' had been around when humans entered the atomic age. Oh wait, we probably wouldn't have. I wish government would keep us all safer.

      1 reply
      0
      None
      AndrewA167Bridges-PdP

      Reply 3 days ago

      I do have to say that this instructable was well written about a subject and device few know about; where it falls down a bit is in it's cavalier attitude on handling a radioactive source, and the ignoring of laws that exist in almost every country about handling such sources.

      It does do some diligence in noting to use some safety equipment to extract the Americium source from a smoke detector, I will give the author that. It also notes the elevated danger such a source possesses should it be ingested. But it might have gone further to warn people that what they are doing may be subject to laws in their country, and that proceeding could open them to legal liability.

      Regarding your assertion that humans would not have "entered the atomic age" had the dangers been known, I would dispute that. I think, had we known the dangers, we would have proceeded far more cautiously than we did, and many of the accidents that were suffered by researchers and others throughout the early to post-WW2 years may have been avoided.

      There's also the (slim) possibility we, as a species, would have not proceeded with the development of nuclear weapons; one can hardly say we have developed socially or responsibly enough to handle weapons which can cause an existential crisis to our species should they be used en-masse. While so far, their existence have seemed to have deterred wars of the scale we have seen in the past, less than a century is not anywhere near long enough of a time to know if the reasoning of MAD holds true long-term. Given that our current POTUS has in the past ruminated on why we shouldn't be able to use such weapons, it seems clear that it is only a matter of time before some country actually does so. This would seem to indicate that we have learned little to nothing regarding these weapons as a species, unfortunately.

      The government regulations we have in place currently for handling radioactive material were arrived at precisely because such material is now known to be dangerous in the hands of those who either do not or can not handle it responsibly. Whether that is individuals, companies, or nation-states does not matter; these regulations seek to try to control such proliferation in order to help, in whatever manner, to keep people safe.

      That is part of the role of government; it is why government as a concept exists, period - it is power, willingly or unwillingly ceded to an entity in the idea and hope that such entity will keep the "citizens" from harm. One can argue that there is a point where doing so does in fact constitute a harm to the citizens; but you need to make such an argument for it to be considered, which you haven't.

      I'd argue that in this case, the laws and regulations that surround the handling of nuclear material from our governments around the world have been an attempt to keep the citizenry safer, and that such regulation does not rise to a harm itself.